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On testing quality and traceability of virgin olive oil by calorimetry
Authors: Angiuli, M.; Ferrari, C.; Lepori, L.; Matteoli, E.; Salvetti, G.;
Tombari, E.; Banti, A.; Minnaja, N.
April 2006
Extra Virgin olive oils (7 samples) originating from different areas of
Tuscany, defective olive oils (5 samples), commercial edible seed oils (4
samples) and two commercial samples of olive oil (one declared 'extra virgin
olive oil' and one 'olive oil') were studied by different calorimetric
techniques: high sensitivity isothermal, differential scanning, and
modulated scanning calorimetry. The temperature interval (-60) - (+30)°C was
explored for monitoring: i) the main features of the liquid<->solid phase
transitions, ii) the nucleation and growth rate of the polymorphous
crystalline phases of the triacylglicerols, and iii) the melting process.
This investigation was planned for verifying the utility and effectiveness
of calorimetry for screening quality and origin of olive oil. To this end,
the main calorimetric operation modes have been applied, the experimental
results reported and their utility for developing an effective and reliable
screening protocol discussed. © 2006 Akademiai Kiado.